Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL7-1 |
| Synchrotron site | SSRL |
| Beamline | BL7-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-12-02 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9805, 0.9919, 0.9809 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 26.550, 59.584, 159.473 |
| Unit cell angles | 90.00, 91.56, 90.00 |
Refinement procedure
| Resolution | 33.130 - 2.600 |
| R-factor | 0.2622 |
| Rwork | 0.260 |
| R-free | 0.28770 |
| Structure solution method | MAD |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.614 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | PHENIX |
| Refinement software | REFMAC (5.6.0074) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 50.000 | 50.000 | 2.690 |
| High resolution limit [Å] | 2.600 | 5.600 | 2.600 |
| Rmerge | 0.058 | 0.032 | 0.269 |
| Number of reflections | 15096 | ||
| <I/σ(I)> | 13 | 3.98 | |
| Completeness [%] | 97.5 | 97.2 | 93.2 |
| Redundancy | 3.6 | 3.9 | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.2 | 298 | PEG MME 2K, pH 7.2, vapor diffusion, temperature 298K |
