3NLL

CLOSTRIDIUM BEIJERINCKII FLAVODOXIN MUTANT: G57A OXIDIZED

Experimental procedure

Detector technology	AREA DETECTOR
Spacegroup name	P 31 2 1
Unit cell lengths	61.480, 61.480, 70.290
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 2.400
R-factor	0.15
Rwork	0.150
RMSD bond length	0.010
RMSD bond angle	23.890 *
Data reduction software	SDMS (DETECTOR SYSTEM (NIELSEN))
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall
High resolution limit [Å]	2.400 *
Rmerge	0.025 *
Completeness [%]	96.1 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	6.8 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ammonium sulfate	2.5-2.8 (M)
2	1	reservoir	Tris-HCl		or phosphate