3NAA
Crystal structure of Fab15 Mut5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-17 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.534, 74.784, 65.198 |
Unit cell angles | 90.00, 103.50, 90.00 |
Refinement procedure
Resolution | 30.559 - 1.700 |
R-factor | 0.1791 |
Rwork | 0.178 |
R-free | 0.19990 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3na9 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.094 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.6.1_357)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.559 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.073 | 0.423 |
Number of reflections | 55410 | |
<I/σ(I)> | 8.7 | 1.8 |
Completeness [%] | 98.9 | 98.3 |
Redundancy | 3.61 | 3.01 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |