3N9M
ceKDM7A from C.elegans, alone
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-17A |
| Synchrotron site | Photon Factory |
| Beamline | BL-17A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-03-29 |
| Detector | RAYONIX MX-225 |
| Wavelength(s) | 1.0000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 66.004, 144.515, 78.413 |
| Unit cell angles | 90.00, 106.69, 90.00 |
Refinement procedure
| Resolution | 32.685 - 2.493 |
| R-factor | 0.2038 |
| Rwork | 0.201 |
| R-free | 0.24700 |
| Structure solution method | SAD |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.871 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.590 |
| High resolution limit [Å] | 2.493 | 2.493 |
| Total number of observations | 269550 | |
| Number of reflections | 48134 | |
| Completeness [%] | 98.4 | 95.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.6 | 277 | 18% PEG 10000, 0.1M Bis-Tris, pH 6.6, 0.2M Sodium Formate, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
