3N4T

apo APH(2")-IVa form I

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL9-1
Synchrotron site	SSRL
Beamline	BL9-1
Temperature [K]	100
Detector technology	CCD
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9795
Spacegroup name	P 21 21 21
Unit cell lengths	50.060, 63.610, 101.340
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.800 - 2.200
R-factor	0.1899
Rwork	0.187
R-free	0.24290
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.011
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	MOLREP
Refinement software	PHENIX ((phenix.refine: 1.5_2))

Data quality characteristics

	Overall
Low resolution limit [Å]	29.800
High resolution limit [Å]	2.200
Rmerge	0.060
Number of reflections	16673
<I/σ(I)>	17.2
Completeness [%]	97.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1