3N4P

Human cytomegalovirus terminase nuclease domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Wavelength(s)	1.000
Spacegroup name	P 21 21 21
Unit cell lengths	82.860, 87.960, 188.380
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.990 - 2.150
R-factor	0.2219
Rwork	0.219
R-free	0.27201
Structure solution method	SIRAS
RMSD bond length	0.023
RMSD bond angle	2.119
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	SHARP
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	98.700	2.200
High resolution limit [Å]	2.150	2.150
Number of reflections	72855
<I/σ(I)>	11.5	2.6
Completeness [%]	96.3	91.1
Redundancy	6	4.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1
1