3MYE
Crystal Structure of HP67 L61GL
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU300 |
| Temperature [K] | 200 |
| Detector technology | IMAGE PLATE |
| Collection date | 2009-11-24 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 29.830, 40.240, 51.555 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 14.915 - 1.799 |
| R-factor | 0.1804 |
| Rwork | 0.178 |
| R-free | 0.19930 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.995 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((phenix.refine: 1.6_289)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 14.915 | 1.980 |
| High resolution limit [Å] | 1.799 | 1.799 |
| Number of reflections | 5971 | |
| Completeness [%] | 97.6 | 97 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.2 M Sodium Acetate, 0.1 M Cacodylate, 30% Polyethylene Glycol 10,000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
