3M9Q
Drosophila MSL3 chromodomain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Wavelength(s) | 1.0000 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 60.407, 60.407, 113.805 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.710 - 1.290 |
R-factor | 0.171 |
Rwork | 0.170 |
R-free | 0.19200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2f5k |
RMSD bond length | 0.008 |
RMSD bond angle | 1.156 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASES |
Refinement software | REFMAC (5.4.0069) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.340 |
High resolution limit [Å] | 1.290 | 2.780 | 1.290 |
Rmerge | 0.078 | 0.063 | 0.301 |
Number of reflections | 60843 | ||
<I/σ(I)> | 13.6 | ||
Completeness [%] | 99.0 | 97.9 | 95.4 |
Redundancy | 8.1 | 7.7 | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 283 | 0.2M Sodium acetate, 16% Polyethylene glycol-3350, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 283K |