3M8W
Phosphopentomutase from Bacillus cereus
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-G |
| Synchrotron site | APS |
| Beamline | 21-ID-G |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 0.979 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 91.238, 76.552, 106.561 |
| Unit cell angles | 90.00, 108.89, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.850 |
| R-factor | 0.1582 |
| Rwork | 0.157 |
| R-free | 0.18570 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.080 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.700 | 1.920 |
| High resolution limit [Å] | 1.850 | 1.850 |
| Number of reflections | 116902 | |
| <I/σ(I)> | 13.3 | 3 |
| Completeness [%] | 98.6 | 99.1 |
| Redundancy | 3.1 | 2.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
