3M76
Crystal Structure of Plant SLAC1 homolog TehA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-11-01 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | H 3 |
Unit cell lengths | 95.673, 95.673, 136.270 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.000 - 1.500 |
R-factor | 0.13 |
Rwork | 0.129 |
R-free | 0.14900 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.014 |
RMSD bond angle | 1.689 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.530 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.053 | 0.530 |
Number of reflections | 74134 | |
<I/σ(I)> | 13 | |
Completeness [%] | 99.3 | 86 |
Redundancy | 6.5 | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.8 | 298 | 28% PEG600, 50mM Hepe-Na pH7.8, 1mM ZnSO4, vapor diffusion, hanging drop, temperature 298K |