3M75
Crystal Structure of Plant SLAC1 homolog TehA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-01-01 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | H 3 |
Unit cell lengths | 96.588, 96.588, 135.904 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.000 - 1.600 |
R-factor | 0.148 |
Rwork | 0.147 |
R-free | 0.16800 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.010 |
RMSD bond angle | 1.273 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.075 | 0.856 |
Number of reflections | 61416 | |
<I/σ(I)> | 7.6 | 2.5 |
Completeness [%] | 98.5 | 99.9 |
Redundancy | 3.8 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.8 | 298 | 28% PEG600, 50mM Hepe-Na pH7.8, 1mM ZnSO4, temperature 298K, VAPOR DIFFUSION, HANGING DROP |