Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X4A |
| Synchrotron site | NSLS |
| Beamline | X4A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-10-17 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.97915 |
| Spacegroup name | P 1 |
| Unit cell lengths | 33.648, 42.720, 50.448 |
| Unit cell angles | 65.85, 77.41, 69.82 |
Refinement procedure
| Resolution | 22.130 - 1.300 |
| R-factor | 0.12544 |
| Rwork | 0.124 |
| R-free | 0.15545 |
| Structure solution method | SAD |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.761 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | PHENIX |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 22.130 |
| High resolution limit [Å] | 1.300 |
| Rmerge | 0.081 |
| Number of reflections | 37566 |
| Completeness [%] | 67.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 10% PEG 3350, 0.2M sodium formate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K |
