3M38
The roles of Glutamates and Metal ions in a rationally designed nitric oxide reductase based on myoglobin: I107E FeBMb (No metal ion binding to FeB site)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X12C |
| Synchrotron site | NSLS |
| Beamline | X12C |
| Detector technology | CCD |
| Collection date | 2009-02-24 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1.0890 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 39.850, 46.980, 77.670 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 1.420 |
| Structure solution method | AB INITIO |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.026 |
| Phasing software | SHELX |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 40.950 |
| High resolution limit [Å] | 1.420 |
| Rmerge | 0.041 |
| Number of reflections | 24766 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
