3LS7
Crystal structure of Thermolysin in complex with Xenon
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2009-02-08 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 93.100, 93.100, 130.200 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 1.980 |
R-factor | 0.176 |
Rwork | 0.165 |
R-free | 0.23400 |
Structure solution method | AB INITIO |
Starting model (for MR) | NONE |
RMSD bond length | 0.007 |
RMSD bond angle | 0.022 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | HKL2Map |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.020 |
High resolution limit [Å] | 1.980 | 1.980 |
Number of reflections | 23786 | |
<I/σ(I)> | 35.2 | 35.2 |
Completeness [%] | 99.7 | 98.6 |
Redundancy | 24.1 | 19.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 288 | 50 mM Tris/HCl, 50 % DMSO, 1.8 M CsCl, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 288K |