Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 200 |
| Detector technology | CCD |
| Collection date | 2003-03-11 |
| Detector | SBC-3 |
| Wavelength(s) | 0.96367 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 52.020, 139.610, 156.000 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 49.350 - 2.500 |
| R-factor | 0.19704 |
| Rwork | 0.195 |
| R-free | 0.22905 |
| Structure solution method | MAD |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.447 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.590 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Rmerge | 0.064 | 0.440 |
| Number of reflections | 40218 | |
| <I/σ(I)> | 8 | 2.1 |
| Completeness [%] | 99.8 | 99.3 |
| Redundancy | 4.48 | 4.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7 | 290 | SODIUM CHLORIDE, SODIUM FORMATE, GLYCEROL, PH 7, VAPOR DIFFUSION, TEMPERATURE 290K |
| 1 | VAPOR DIFFUSION | 7 | 290 | SODIUM CHLORIDE, SODIUM FORMATE, GLYCEROL, PH 7, VAPOR DIFFUSION, TEMPERATURE 290K |
