3LLI

Sulfhydryl Oxidase Fragment of Human QSOX1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RUH3R
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2008-07-11
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.5418
Spacegroup name	P 64 2 2
Unit cell lengths	85.606, 85.606, 125.706
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	50.000 - 2.050
Rwork	0.275
R-free	0.32450
RMSD bond length	0.011
RMSD bond angle	1.725
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	SOLVE
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.120
High resolution limit [Å]	2.050	2.050
Number of reflections	17724
<I/σ(I)>	16.4	2.6
Completeness [%]	99.8	98.1
Redundancy	16	11.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	12-16% (w/v) PEG 8000, 0.1M Citric acid, pH 5.3-5.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K