3LCJ
Phosphopantetheine adenylyltransferase from Mycobacterium tuberculosis complexed with CoA
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | BRUKER AXS MICROSTAR |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Wavelength(s) | 1.54 |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 98.839, 98.839, 112.884 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 12.000 - 2.100 |
| R-factor | 0.22855 |
| Rwork | 0.227 |
| R-free | 0.25932 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.254 |
| Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 96.810 |
| High resolution limit [Å] | 2.100 |
| Number of reflections | 9684 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
