3L8L

Gramicidin D complex with sodium iodide

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 5ID-B
Synchrotron site	APS
Beamline	5ID-B
Temperature [K]	100
Detector technology	CCD
Collection date	2000
Detector	MAR CCD 165 mm
Spacegroup name	P 21 21 21
Unit cell lengths	29.816, 31.255, 51.667
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	26.740 - 1.250
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1w5u
RMSD bond length	0.015
RMSD bond angle	0.035
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	SHELXL-97

Data quality characteristics

	Overall
Low resolution limit [Å]	26.740
High resolution limit [Å]	1.250
Number of reflections	19883

Crystallization Conditions

crystal ID	method	pH	temperature	details
1				BATCH CRYSTALLIZATION WITH 30 MG/ML GRAMICIDIN AND SATURATED NAI IN METHANOL