3L7W
The Crystal Structure of smu.1704 from Streptococcus mutans UA159
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BSRF BEAMLINE 3W1A |
Synchrotron site | BSRF |
Beamline | 3W1A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-01-19 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.9790 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 57.070, 57.070, 174.920 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 18.851 - 2.200 |
R-factor | 0.2106 |
Rwork | 0.204 |
R-free | 0.26940 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.206 |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.300 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 9136 | |
Completeness [%] | 98.9 | 93.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 289 | 0.1M HEPES pH7.5, 3.0M Sodium chloride, VAPOR DIFFUSION, SITTING DROP, temperature 289K |