3L7Q
Crystal structure of AldR from streptococcus mutans
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-002 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-07-20 |
| Detector | RIGAKU SATURN 944 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 171.124, 78.182, 102.488 |
| Unit cell angles | 90.00, 121.28, 90.00 |
Refinement procedure
| Resolution | 41.370 - 2.500 |
| R-factor | 0.21651 |
| Rwork | 0.215 |
| R-free | 0.24974 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1qd9 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.367 |
| Data reduction software | CrystalClear |
| Data scaling software | CrystalClear |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.590 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Number of reflections | 40167 | |
| Completeness [%] | 99.9 | 99 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 0.2M MgCl2, 0.1M Tris-HCl pH8.5, 25.0% PEG3350, VAPOR DIFFUSION, SITTING DROP |
