3L75
Cytochrome BC1 complex from chicken with fenamidone bound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-07-30 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.00 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 172.285, 182.141, 241.198 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 58.780 - 2.790 |
R-factor | 0.248 |
Rwork | 0.248 |
R-free | 0.27500 |
Structure solution method | RIGID BODY REFINEMENT |
Starting model (for MR) | 3h1h |
RMSD bond length | 0.008 |
RMSD bond angle | 1.300 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 99.000 | 2.830 |
High resolution limit [Å] | 2.700 | 2.780 |
Number of reflections | 186451 | |
<I/σ(I)> | 20.5 | 0.725 |
Completeness [%] | 97.9 | 69.2 |
Redundancy | 5.7 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.77 | 277 | FINAL CONCENTRATIONS BEFORE DIFFUSION: 50 MM CACODYLATE, 9.4 MM TRISHCL, 10 MM MGCL2, 50 G/L GLYCEROL, 30 G/L PEG 3350DA, 0.23 MM EDTA, 0.47 G/L UNDECYL MALTOSIDE, 31 MM OCTYL GLUCOSIDE, PH 6.77, VAPOR DIFFUSION, SITTING DROP, temperature 277K |