3L74
Cytochrome BC1 complex from chicken with famoxadone bound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-07-28 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 171.893, 181.687, 240.750 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 58.660 - 2.760 |
R-factor | 0.259 |
Rwork | 0.259 |
R-free | 0.28600 |
Structure solution method | RIGID BODY REFINEMENT |
Starting model (for MR) | 3h1h |
RMSD bond length | 0.008 |
RMSD bond angle | 1.300 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 99.000 | 2.740 |
High resolution limit [Å] | 2.700 | 2.700 |
Number of reflections | 201091 | |
<I/σ(I)> | 17.8 | 0.891 |
Completeness [%] | 95.9 | 66 |
Redundancy | 3.3 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.77 | 273 | FINAL CONCENTRATIONS BEFORE DIFFUSION: 50 MM CACODYLATE, 9.4 MM TRISHCL, 10 MM MGCL2, 50 G/L GLYCEROL, 30 G/L PEG 3350DA, 0.23 MM EDTA, 0.47 G/L UNDECYL MALTOSIDE, 31 MM OCTYL GLUCOSIDE, PH 6.77 , VAPOR DIFFUSION, SITTING DROP, temperature 273K |