3L73
Cytochrome BC1 complex from chicken with triazolone inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-08-26 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 171.499, 182.934, 241.028 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.970 - 3.040 |
R-factor | 0.2597 |
Rwork | 0.259 |
R-free | 0.29300 |
Structure solution method | RIGID BODY REFINEMENT |
Starting model (for MR) | 3h1h |
RMSD bond length | 0.009 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.950 |
High resolution limit [Å] | 2.900 | 2.900 |
Number of reflections | 167200 | |
<I/σ(I)> | 19.38 | 1.072 |
Completeness [%] | 99.9 | 99.7 |
Redundancy | 4.3 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.77 | 277 | FINAL CONCENTRATIONS BEFORE DIFFUSION: 50 MM CACODYLATE, 9.4 MM TRISHCL, 10 MM MGCL2, 50 G/L GLYCEROL, 30 G/L PEG 3350DA, 0.23 MM EDTA, 0.47 G/L UNDECYL MALTOSIDE, 31 MM OCTYL GLUCOSIDE, PH 6.77, VAPOR DIFFUSION, SITTING DROP, temperature 277K |