Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2007-10-29 |
| Detector | MAR scanner 345 mm plate |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 69.644, 62.165, 69.935 |
| Unit cell angles | 90.00, 113.99, 90.00 |
Refinement procedure
| Resolution | 34.650 - 1.740 |
| R-factor | 0.18182 |
| Rwork | 0.180 |
| R-free | 0.20737 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.610 |
| Refinement software | REFMAC (5.6.0041) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 34.650 | 1.790 |
| High resolution limit [Å] | 1.740 | 1.750 |
| Number of reflections | 53875 | |
| <I/σ(I)> | 12.6 | 1.4 |
| Completeness [%] | 97.6 | 80 |
| Redundancy | 4.9 | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 300 | 0.1M Tris-HCl pH 8.0, 1.8M (NH4)2SO4, VAPOR DIFFUSION, SITTING DROP, temperature 300.0K |
