3L0J
Crystal structure of orphan nuclear receptor RORgamma in complex with natural ligand
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-F |
| Synchrotron site | APS |
| Beamline | 21-ID-F |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 58.502, 58.502, 159.032 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 39.280 - 2.400 |
| R-factor | 0.19712 |
| Rwork | 0.193 |
| R-free | 0.28295 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.565 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.400 |
| Number of reflections | 11412 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
