3KUF
The Crystal Structure of the Tudor Domains from FXR1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Collection date | 2009-11-05 |
Wavelength(s) | 1.0 |
Spacegroup name | H 3 |
Unit cell lengths | 73.102, 73.102, 94.412 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 26.290 - 2.700 |
R-factor | 0.24986 |
Rwork | 0.248 |
R-free | 0.29577 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3h8z |
RMSD bond length | 0.008 |
RMSD bond angle | 0.880 |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 26.290 |
High resolution limit [Å] | 2.700 |
Number of reflections | 5131 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |