3KTK
Structure of ClpP in complex with ADEP2 in triclinic crystal form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 4A |
| Synchrotron site | PAL/PLS |
| Beamline | 4A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-03-03 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1.0000 |
| Spacegroup name | P 1 |
| Unit cell lengths | 97.171, 97.241, 100.035 |
| Unit cell angles | 71.51, 73.89, 77.30 |
Refinement procedure
| Resolution | 50.000 - 2.600 |
| Rwork | 0.269 |
| R-free | 0.29400 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.139 |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.600 |
| Number of reflections | 97687 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | hanging drop | 9.5 | 295 | 0.1M CHES, 200mM NaCl, 10% PEG 8000, pH 9.5, hanging drop, temperature 295K |
