3KOD
DTD from Plasmodium falciparum in complex with D-Serine
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2008-10-22 |
| Detector | MAR scanner 345 mm plate |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 |
| Unit cell lengths | 52.281, 55.147, 92.535 |
| Unit cell angles | 106.86, 101.86, 94.45 |
Refinement procedure
| Resolution | 30.000 - 3.000 |
| R-factor | 0.203 |
| Rwork | 0.197 |
| R-free | 0.30500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.502 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 3.010 |
| High resolution limit [Å] | 2.910 | 2.910 |
| Rmerge | 0.064 | 0.566 |
| Number of reflections | 20428 | |
| <I/σ(I)> | 10.3 | |
| Completeness [%] | 97.0 | 89.8 |
| Redundancy | 2.9 | 2.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 25% PEG 3350, 0.1M MES, pH 6.2-6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
