3KGK
Crystal structure of ArsD
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 32-ID |
| Synchrotron site | APS |
| Beamline | 32-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-07-13 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 37.841, 73.774, 41.248 |
| Unit cell angles | 90.00, 97.30, 90.00 |
Refinement procedure
| Resolution | 35.780 - 1.400 |
| R-factor | 0.19348 |
| Rwork | 0.192 |
| R-free | 0.21912 |
| Structure solution method | SAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.157 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.5.0046) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.900 | 1.520 |
| High resolution limit [Å] | 1.400 | 1.400 |
| Number of reflections | 43232 | |
| <I/σ(I)> | 16 | 3.1 |
| Completeness [%] | 97.9 | 97.3 |
| Redundancy | 4.2 | 4.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293 | 25% PEG 6000, 0.1 M calcium acetate, 0.1 M HEPES, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
