3K9Z
Rational Design of a Structural and Functional Nitric Oxide Reductase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X12C |
| Synchrotron site | NSLS |
| Beamline | X12C |
| Temperature [K] | 298 |
| Detector technology | CCD |
| Collection date | 2009-08-20 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1.7309 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 39.600, 48.240, 77.480 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 1.720 |
| Rwork | 0.243 |
| Structure solution method | AB INITIO |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.962 |
| Phasing software | SHELX |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.780 |
| High resolution limit [Å] | 1.720 | 1.720 |
| Number of reflections | 13961 | |
| Completeness [%] | 98.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 7 | 298 | pH 7, EVAPORATION, temperature 298K |
