3K0G
Crystal Structure of CNG mimicking NaK mutant, NaK-ETPP, Na+ complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Detector technology | CCD |
| Spacegroup name | I 4 |
| Unit cell lengths | 67.570, 67.570, 89.539 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - 1.950 |
| Rwork | 0.204 |
| R-free | 0.22800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.516 |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 1.950 |
| Number of reflections | 14710 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | MPD, NaCl, pH 6.5-8.5, vapor diffusion, temperature 293K |
