3JZN

Structure of EED in apo form

Experimental procedure

Source type	ROTATING ANODE
Source details	RIGAKU
Temperature [K]	100
Wavelength(s)	1.7
Spacegroup name	P 21 21 21
Unit cell lengths	57.640, 85.159, 91.327
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	62.280 - 2.600
R-factor	0.17509
Rwork	0.172
R-free	0.23905
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.016
RMSD bond angle	1.619
Refinement software	REFMAC (5.5.0072)

Data quality characteristics

	Overall
Low resolution limit [Å]	62.300
High resolution limit [Å]	2.600
Number of reflections	12215
Completeness [%]	89.3
Redundancy	5.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.5		3.5 mM NaF, 10 mM TCEP, 15% Glycerol, pH 7.5, VAPOR DIFFUSION, SITTING DROP