3JVB
Crystal structure of infectious baculovirus polyhedra
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-04-05 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 1.0 |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 102.437, 102.437, 102.437 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.910 - 2.170 |
| R-factor | 0.164 |
| Rwork | 0.161 |
| R-free | 0.18990 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3jw6 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.040 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SHARP |
| Refinement software | BUSTER (2.8.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.290 |
| High resolution limit [Å] | 2.170 | 2.170 |
| Rmerge | 0.349 | |
| Number of reflections | 9646 | |
| <I/σ(I)> | 8 | 2.3 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 15 | 14.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | 300 | Natural intracellular Crystals were directly purified from larvae of porina moths infected by a baculovirus (WNPV), pH 7, temperature 300K |
