3IWL
Crystal structure of cisplatin bound to a human copper chaperone (monomer)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-B |
Synchrotron site | APS |
Beamline | 23-ID-B |
Temperature [K] | 113 |
Detector technology | CCD |
Collection date | 2009-04-01 |
Detector | MARRESEARCH |
Wavelength(s) | 0.90511 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 54.070, 54.070, 55.578 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.830 - 1.600 |
R-factor | 0.181 |
Rwork | 0.179 |
R-free | 0.21000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.252 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.5.0088) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.600 |
Number of reflections | 13182 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 294 | 2M lithium sulfate, 0.1M MES, pH 6, VAPOR DIFFUSION, HANGING DROP, temperature 294K |