Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.2.2 |
| Synchrotron site | ALS |
| Beamline | 8.2.2 |
| Temperature [K] | 200 |
| Detector technology | CCD |
| Collection date | 2003-07-20 |
| Detector | ADSC QUANTUM 4 |
| Spacegroup name | P 42 21 2 |
| Unit cell lengths | 100.120, 100.120, 30.090 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 1.600 |
| R-factor | 0.144 |
| Rwork | 0.144 |
| R-free | 0.20000 |
| Structure solution method | AB INITIO |
| Starting model (for MR) | 1lu4 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 0.034 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | EPMR |
| Refinement software | SHELXL |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.660 |
| High resolution limit [Å] | 1.600 | 1.600 |
| Rmerge | 0.068 | 0.597 |
| Number of reflections | 23073 | |
| <I/σ(I)> | 40.68 | 3.85 |
| Completeness [%] | 100.0 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | 298 | 0.1 M NA malonate ph 7.0, 2.04 M NA citrate, 5% LDAO, temperature 298K |
