3INS
STRUCTURE OF INSULIN. RESULTS OF JOINT NEUTRON AND X-RAY REFINEMENT
Experimental procedure
| Spacegroup name | H 3 |
| Unit cell lengths | 82.500, 82.500, 34.000 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | ? - 2.200 |
| R-factor | 0.182 * |
| RMSD bond length | 0.019 |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 10.000 * |
| High resolution limit [Å] | 1.500 * |
| Total number of observations | 13476 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 6.5 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | d6-acetone | 30 (%) | |
| 2 | 1 | 1 | 70 (%) | ||
| 3 | 1 | 1 | sodium citrate | 0.1 (M) | |
| 4 | 1 | 1 | zinc chloride | 0.005 (%) |
