3ILB
Crystal structure of mouse Bcl-xl mutant (R139A) at pH 6.0
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 6C1 |
Synchrotron site | PAL/PLS |
Beamline | 6C1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-10-08 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 52.497, 34.721, 95.552 |
Unit cell angles | 90.00, 89.62, 90.00 |
Refinement procedure
Resolution | 35.450 - 2.380 |
R-factor | 0.2394 |
Rwork | 0.237 |
R-free | 0.29340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1pq0 |
RMSD bond length | 0.020 |
RMSD bond angle | 1.768 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.470 |
High resolution limit [Å] | 2.380 | 2.380 |
Rmerge | 0.140 | 0.140 |
Number of reflections | 12366 | |
<I/σ(I)> | 25 | 4.5 |
Completeness [%] | 91.1 | 91.4 |
Redundancy | 4 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 295 | 1.2M Ammonium sulphate, 0.3M Lithium sulphate, MES, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 295K |