3IDE
Structure of IPNV subviral particle
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-06-28 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 0.9500 |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 303.431, 303.431, 303.431 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 29.754 - 3.350 |
| R-factor | 0.218 |
| Rwork | 0.217 |
| R-free | 0.23340 |
| Structure solution method | SIRAS |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.918 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 30.000 | 30.000 | 3.470 |
| High resolution limit [Å] | 3.350 | 7.190 | 3.350 |
| Rmerge | 0.080 | 0.054 | 0.379 |
| Number of reflections | 66153 | ||
| <I/σ(I)> | 16.1 | 3.3 | |
| Completeness [%] | 99.7 | 99.7 | 98.3 |
| Redundancy | 4.5 | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 4.6 | 293 | 1M 1,6-hexanediol, 10mM CoCl2, 100mM sodium acetate pH 4.6, VAPOR DIFFUSION, temperature 293K |
