3I7G

MMP-13 in complex with a non zinc-chelating inhibitor

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Detector technology	CCD
Detector	MARMOSAIC 225 mm CCD
Spacegroup name	C 1 2 1
Unit cell lengths	133.770, 36.100, 95.333
Unit cell angles	90.00, 130.77, 90.00

Refinement procedure

Resolution	33.374 - 1.950
R-factor	0.176
Rwork	0.173
R-free	0.22800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.237
Refinement software	PHENIX (1.4_6)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.650
High resolution limit [Å]	1.950
Number of reflections	24419

Crystallization Conditions

crystal ID	method	pH	temperature	details
1