Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE A1 |
| Synchrotron site | CHESS |
| Beamline | A1 |
| Temperature [K] | 100 |
| Collection date | 2005-11-05 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 187.415, 101.687, 94.751 |
| Unit cell angles | 90.00, 119.75, 90.00 |
Refinement procedure
| Resolution | 43.230 - 3.100 |
| Rwork | 0.244 |
| R-free | 0.31710 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2OVK |
| RMSD bond length | 0.014 |
| RMSD bond angle | 2.443 |
| Data scaling software | HKL-2000 |
| Phasing software | AMoRE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 43.230 | 3.210 |
| High resolution limit [Å] | 3.100 | 3.100 |
| Rmerge | 0.111 | 0.287 |
| Number of reflections | 25326 | |
| <I/σ(I)> | 10.2 | 2.1 |
| Completeness [%] | 88.8 | 41.5 |
| Redundancy | 3.9 | 1.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
