3HYU
Crystal structure of the altitude adapted hemoglobin of guinea pig.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR-H |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2009-03-06 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 83.540, 89.950, 82.720 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.590 - 1.670 |
R-factor | 0.179 |
Rwork | 0.177 |
R-free | 0.20300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2d5x |
RMSD bond length | 0.011 |
RMSD bond angle | 1.165 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.1.4) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.590 | 1.710 |
High resolution limit [Å] | 1.670 | 1.670 |
Rmerge | 0.052 | 0.255 |
Number of reflections | 36376 | 2466 |
<I/σ(I)> | 35.8 | 9.95 |
Completeness [%] | 99.7 | 92 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | hanging drop | 6.5 | 298 | Sodium Phosphate, Ammonia Sulfate, pH 6.5, hanging drop, temperature 298K |