3HVE

Structures of SPOP-Substrate Complexes: Insights into Molecular Architectures of BTB-Cul3 Ubiquitin Ligases: GigaxoninBTB/3-box

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.2
Synchrotron site	ALS
Beamline	8.2.2
Collection date	2007-04-13
Wavelength(s)	0.9794
Spacegroup name	P 1 21 1
Unit cell lengths	46.480, 55.600, 120.600
Unit cell angles	90.00, 91.10, 90.00

Refinement procedure

Resolution	50.000 - 2.800
Rwork	0.302
R-free	0.33300
Structure solution method	SAD
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SOLVE
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	100.000	2.900
High resolution limit [Å]	2.800	2.800
Number of reflections	15314
<I/σ(I)>	20.8	5.3
Redundancy	3.2	2.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1