3HQ8
CcpA from G. sulfurreducens S134P/V135K variant
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X12 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X12 |
| Detector technology | CCD |
| Collection date | 2008-07-27 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1.05 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 56.160, 89.508, 75.111 |
| Unit cell angles | 90.00, 107.57, 90.00 |
Refinement procedure
| Resolution | 44.770 - 2.400 |
| R-factor | 0.23418 |
| Rwork | 0.229 |
| R-free | 0.32447 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3hq6 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.685 |
| Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 70.000 |
| High resolution limit [Å] | 2.400 |
| Number of reflections | 27650 |
| <I/σ(I)> | 6.3 |
| Completeness [%] | 98.7 |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
