3HP7
Putative hemolysin from Streptococcus thermophilus.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-05-29 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.958, 81.713, 95.537 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.400 - 1.530 |
R-factor | 0.147 |
Rwork | 0.145 |
R-free | 0.17700 |
Structure solution method | SAD |
RMSD bond length | 0.019 |
RMSD bond angle | 1.727 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELXD |
Refinement software | REFMAC (5.5.0054) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.400 | 1.560 |
High resolution limit [Å] | 1.530 | 1.530 |
Rmerge | 0.067 | 0.681 |
Number of reflections | 54173 | |
<I/σ(I)> | 55.624 | 2.07 |
Completeness [%] | 100.0 | 99.7 |
Redundancy | 12.5 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 289 | 0.1 M Tris buffer, 20% ethanol, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 289K |