3HNS
CS-35 Fab Complex with Oligoarabinofuranosyl Hexasaccharide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-01-28 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.115872 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 146.725, 96.234, 36.065 |
Unit cell angles | 90.00, 102.35, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.070 | 0.223 |
Number of reflections | 29618 | |
<I/σ(I)> | 10.8 | 3.4 |
Completeness [%] | 94.5 | 74.6 |
Redundancy | 3.3 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.1 | 295 | sodium citrate, magnesium chloride, TMAO, pH 7.1, VAPOR DIFFUSION, HANGING DROP, temperature 295K |