3H9C
Structure of methionyl-tRNA synthetase: crystal form 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-03-19 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.980 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 78.890, 45.400, 86.210 |
Unit cell angles | 90.00, 107.30, 90.00 |
Refinement procedure
Resolution | 29.540 - 1.400 |
R-factor | 0.167 |
Rwork | 0.165 |
R-free | 0.19100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3h97 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.055 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | CNS |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.500 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.057 | 0.300 |
Number of reflections | 109028 | 19290 |
<I/σ(I)> | 11.4 | 2.9 |
Completeness [%] | 94.7 | 90.1 |
Redundancy | 3.1 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.1 | 279 | Ammonium citrate, pH 7.1, VAPOR DIFFUSION, SITTING DROP, temperature 279K |