3GZ6
Crystal structure of Shewanella oneidensis NrtR complexed with a 27mer DNA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | OTHER |
| Collection date | 2008-04-14 |
| Spacegroup name | P 32 1 2 |
| Unit cell lengths | 159.580, 159.580, 73.067 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 33.217 - 2.901 |
| R-factor | 0.1777 |
| Rwork | 0.174 |
| R-free | 0.24720 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3gz5 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.338 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 50.000 | 50.000 | 3.000 |
| High resolution limit [Å] | 2.900 | 6.240 | 2.900 |
| Rmerge | 0.097 | 0.049 | 0.478 |
| Number of reflections | 23259 | ||
| <I/σ(I)> | 20.684 | ||
| Completeness [%] | 98.4 | 98.5 | 97.9 |
| Redundancy | 6.1 | 5.7 | 6.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
