3GW3
human UROD mutant K297N
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-08-18 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 103.073, 103.073, 72.066 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.410 - 1.700 |
R-factor | 0.185 |
Rwork | 0.184 |
R-free | 0.23800 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.533 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 40.000 | 40.000 | 1.760 |
High resolution limit [Å] | 1.700 | 3.660 | 1.700 |
Rmerge | 0.076 | 0.059 | 0.476 |
Number of reflections | 48712 | ||
<I/σ(I)> | 17.191 | ||
Completeness [%] | 99.3 | 99.4 | 96.9 |
Redundancy | 5.3 | 5.7 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | hanging drop | hanging drop |