3GVA

Crystal Structure Analysis of S. Pombe ATL

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 12.3.1
Synchrotron site	ALS
Beamline	12.3.1
Temperature [K]	100
Detector technology	CCD
Collection date	2007-09-15
Detector	ADSC QUANTUM 315
Spacegroup name	P 31 2 1
Unit cell lengths	46.298, 46.298, 169.277
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	39.020 - 2.000
Rwork	0.221
R-free	0.26500
RMSD bond length	0.005
RMSD bond angle	1.100
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	CNS (1.2)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.700
High resolution limit [Å]	2.000	2.000
Rmerge	0.071	0.286
Number of reflections	14855
<I/σ(I)>	25.2	4.9
Completeness [%]	98.7	98.5
Redundancy	9.3	8.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1