3GUD

Crystal structure of a novel intramolecular chaperon

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Detector technology	CCD
Collection date	2008-07-05
Detector	ADSC QUANTUM 4
Spacegroup name	P 3
Unit cell lengths	84.040, 84.040, 41.450
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	42.000 - 2.200
R-factor	0.199
Rwork	0.197
R-free	0.23200
Structure solution method	SIRAS
RMSD bond length	0.009
RMSD bond angle	1.386
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	SHARP
Refinement software	PHENIX ((phenix.refine))

Data quality characteristics

	Overall
Low resolution limit [Å]	42.000
High resolution limit [Å]	2.200
Number of reflections	16515

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		4.8	293	25-30% PEG 2000, 0.1 M NaCitrate pH 4.8, 0.1 M (NH4)2SO4, temperature 293K.